Course

Plantwide Control of Chemical Processes

Indian Institute of Technology Kanpur

This course, "Plantwide Control of Chemical Processes," delves into the critical aspect of control structure selection in chemical process design. It emphasizes:

  • Importance of controlling specific variables and the corresponding manipulated variables.
  • Effective disturbance rejection and profitability maximization in practical operations.
  • Systematic design of plant-wide control systems, even in processes with material/energy recycling.

Course content includes:

  • Essentials of process control: process dynamics, model fitting, PID control, advanced control structures, and multivariable control.
  • Control of common unit operations such as reactors, distillation columns, heat exchangers, and various miscellaneous operations.
  • Plant-wide control fundamentals, including inventory management, the snowball effect, and throughput manipulation.
  • Case studies on processes like the Cumene process and HDA process, highlighting comprehensive control system design.

The course aims to prepare Chemical Engineering students for careers in process operations and offers practicing engineers insights to enhance process efficiency and profitability.

Course Lectures
  • This module serves as an introduction to the course on plantwide control of chemical processes. It outlines the significance of control structure selection in enhancing process efficiency and profitability.

    Key topics include:

    • Overview of control systems in chemical engineering
    • Importance of disturbance rejection
    • Role of the control system designer

    Students will gain insights into the foundational concepts that will be explored in later modules, emphasizing the practical applications of control theory in real-world chemical operations.

  • In this module, we delve into the fundamentals of process dynamics and the concept of negative feedback. Understanding these principles is essential for effective control in chemical processes.

    Topics covered will include:

    • Definition of process dynamics
    • Role of negative feedback in control systems
    • Examples of feedback mechanisms in chemical processes

    Students will learn how feedback can stabilize processes and mitigate disturbances, forming the basis for more advanced control strategies introduced in later modules.

  • Mod-01 Lec-03 PID control
    Dr. Nitin Kaistha

    This module focuses on Proportional-Integral-Derivative (PID) control, a foundational concept in process control. Students will learn about the structure and function of PID controllers.

    Content includes:

    • Understanding PID control theory
    • Application of PID controllers in real-world scenarios
    • Tuning techniques for PID controllers

    Through practical examples, students will gain hands-on experience in tuning PID controllers for optimal performance in chemical processes.

  • This module covers common industrial control loops, as well as advanced control loops. Students will explore various types of control loops used in chemical processes, understanding their design and operational principles.

    Topics include:

    • Basic control loop configurations
    • Advanced loop strategies for complex systems
    • Implementation and troubleshooting of control loops

    By applying this knowledge, students will be prepared to design and utilize control loops effectively in a range of industrial applications.

  • This module continues the discussion on advanced control loops and introduces the concept of multivariable systems. Students will learn how to manage systems with multiple interdependent variables.

    Key points include:

    • Characteristics of multivariable control systems
    • Interaction between different control loops
    • Strategies for effective multivariable control

    Students will engage in practical exercises to understand how to stabilize and optimize multivariable systems in chemical processes.

  • This module introduces systematic tuning methods using frequency domain analysis. Students will learn how to utilize frequency response techniques to tune control systems effectively.

    Topics discussed will include:

    • Overview of frequency domain analysis
    • Techniques for tuning control systems
    • Practical applications in chemical processes

    Students will gain practical skills in analyzing system responses and implementing tuning adjustments to improve overall system performance.

  • This module provides an in-depth understanding of frequency domain analysis, crucial for the design and evaluation of control systems. Students will explore various techniques and tools used in this analysis.

    Key topics include:

    • Fundamentals of frequency response
    • Applications of frequency domain in process control
    • Analysis of system stability and performance

    Through hands-on examples, students will learn to assess system behavior and make data-driven decisions to enhance control strategies.

  • This module focuses on multivariable systems, emphasizing the challenges and strategies for their control. Students will learn how to manage interdependent variables effectively in complex chemical processes.

    Topics covered include:

    • Characteristics of multivariable systems
    • Control strategies for multivariable interactions
    • Case studies of multivariable control applications

    Through practical examples, students will develop skills to optimize control strategies for better process performance.

  • This module discusses Relative Gain Array (RGA) and dynamic decoupling techniques, which are essential for multivariable control systems. Students will explore how to assess and mitigate interactions among control loops.

    Key topics include:

    • Understanding RGA and its applications
    • Dynamic decoupling techniques for improved control
    • Case studies demonstrating RGA in real-world scenarios

    Students will gain insights into how to apply these techniques to enhance control system performance in complex processes.

  • This module introduces model-based control, highlighting its significance in enhancing the performance of chemical processes. Students will learn about different modeling techniques and their applications in control strategy design.

    Topics covered will include:

    • Overview of model-based control concepts
    • Techniques for developing process models
    • Applications of model-based control in chemical engineering

    Through practical examples, students will understand how to leverage models to design effective control systems and improve process outcomes.

  • This module covers Dynamic Matrix Control (DMC), a powerful tool for managing multivariable processes. Students will learn the principles underlying DMC and its practical applications in chemical engineering.

    Key points include:

    • Fundamentals of Dynamic Matrix Control
    • Implementation of DMC in real-world scenarios
    • Benefits of DMC over traditional control methods

    Through case studies, students will gain insights into the effectiveness of DMC in optimizing complex chemical processes.

  • This module focuses on the control of distillation columns, a crucial unit operation in chemical processes. Students will learn about various control strategies tailored for distillation.

    Topics discussed include:

    • Basic principles of distillation control
    • Control techniques for complex column configurations
    • Impact of control on distillation efficiency

    Students will engage in practical exercises to understand how to enhance distillation performance through effective control strategies.

  • This module delves into temperature inferential control within distillation processes. Students will explore how temperature measurements can be used to infer compositions and optimize control.

    Key topics include:

    • Understanding inferential control concepts
    • Techniques for temperature-based composition control
    • Case studies on temperature inferential control applications

    Students will learn how to implement these strategies effectively to improve distillation performance and product quality.

  • This module addresses considerations in temperature inferential control, emphasizing the challenges and best practices in implementing these techniques within distillation processes.

    Topics covered include:

    • Challenges in temperature inferential control
    • Best practices for effective implementation
    • Impact on process stability and product quality

    Through practical examples, students will develop strategies to overcome common issues and enhance the reliability of inferential control systems.

  • This module examines the control of complex column configurations, focusing on advanced strategies for managing intricate distillation systems. Students will learn about specialized control techniques suited for these configurations.

    Key topics include:

    • Types of complex column configurations
    • Control strategies tailored for complex systems
    • Real-world applications and case studies

    Students will gain insights into optimizing control strategies for complex column operations in chemical processes.

  • This module focuses on the control of heat-integrated columns, where energy efficiency is paramount. Students will explore how to manage energy effectively within distillation processes.

    Topics discussed include:

    • Principles of heat integration in distillation
    • Control strategies for managing energy use
    • Case studies on energy-efficient column designs

    Students will engage with practical examples to understand how to enhance energy efficiency while maintaining process performance.

  • This module delves into homogeneous extractive distillation, focusing on its unique control challenges and strategies. Students will learn how to manage the complexities of this advanced distillation method.

    Key topics include:

    • Understanding homogeneous extractive distillation
    • Control challenges and solutions
    • Case studies demonstrating control strategies

    Through practical examples, students will gain insights into optimizing control for improved performance in extractive distillation processes.

  • This module continues the discussion on complex columns, including reactive distillation. Students will explore the unique aspects and control strategies relevant to this advanced distillation method.

    Topics covered include:

    • Overview of reactive distillation principles
    • Control techniques for reactive distillation
    • Case studies on optimizing performance

    Students will engage in practical exercises to understand how to successfully implement control strategies for reactive distillation systems.

  • This module focuses on the control of reactors, a critical unit operation in chemical processes. Students will explore various strategies for managing reactor conditions to ensure optimal performance.

    Topics discussed include:

    • Fundamentals of reactor control
    • Techniques for optimizing reaction conditions
    • Real-world applications and case studies

    Through practical examples, students will learn how to implement effective control strategies to enhance reactor performance.

  • This module continues the discussion on reactor control, focusing on specific types of reactors such as Plug Flow Reactors (PFR) and Continuous Stirred-Tank Reactors (CSTR). Students will learn tailored control strategies for these reactor types.

    Key topics include:

    • Characteristics of PFR and CSTR
    • Control methods specific to each reactor type
    • Challenges and solutions in reactor control

    Through practical exercises, students will develop skills to effectively manage these reactors in various chemical processes.

  • This module explores the intricacies of heat management in Continuous Stirred-Tank Reactors (CSTRs). It delves into the types of heat exchangers used, the importance of maintaining thermal equilibrium, and the strategies for efficient heat removal or addition. The module addresses common challenges such as heat loss, scaling, and fouling, offering solutions to mitigate these issues. It also discusses the role of advanced control strategies in optimizing thermal efficiency and maintaining stability in the face of process variability.

  • This module examines the control mechanisms of heat exchangers and various miscellaneous systems such as compressors and furnaces. It provides insights into the operational parameters essential for maintaining efficiency and how to leverage control systems for optimal performance. The focus is on understanding dynamic responses and adapting control strategies to enhance reliability and profitability. Case studies highlight practical applications and the benefits of integrating advanced process controls in these systems.

  • This module introduces the concept of degrees of freedom in process control, explaining how to identify and analyze them in chemical processes. It covers the impact of degrees of freedom on system flexibility and process constraints. Through examples, learners will understand how to leverage control strategies that effectively utilize available degrees of freedom to enhance process efficiency and stability. The module also discusses troubleshooting techniques for common issues arising from improper degrees of freedom management.

  • This module is a continuation of the previous one, delving deeper into the analysis of degrees of freedom. It focuses on advanced methods for identifying and evaluating degrees of freedom in complex systems. Learners will explore how changes in process conditions affect degrees of freedom and how to recalibrate control systems accordingly. The module includes practical exercises to reinforce concepts and highlights the importance of maintaining a robust control structure for dealing with system variability.

  • This module illustrates the critical considerations in control structure synthesis for chemical processes. It covers topics such as selecting controlled and manipulated variables, balancing complexity with control robustness, and ensuring process safety. Learners will assess different control structure designs through case studies, understanding the trade-offs involved. The module emphasizes the role of systematic design approaches in achieving optimal control solutions that maximize process efficiency and safety while minimizing costs.

  • This module focuses on the two-column recycle process, providing an in-depth analysis of its control challenges and solutions. It covers the principles of recycle operations, the impact on process dynamics, and the methods for achieving effective disturbance rejection. Learners will explore case studies demonstrating successful control strategies and the nuances of integrating recycle streams into plant-wide control systems. The module also highlights the importance of optimizing throughput and minimizing energy consumption.

  • This module addresses the selection of throughput manipulators in chemical processes. It explains the criteria for choosing appropriate manipulators and the impact of these selections on process efficiency and control stability. The module includes practical guidelines for evaluating and implementing throughput manipulation strategies, supported by examples from industry case studies. Learners will gain insights into optimizing process throughput while maintaining control over system variability and disturbances.

  • This module delves into the design of plantwide control structures, emphasizing the integration of unit operations and control loops. It covers the methodologies for developing robust control structures that enhance process safety and profitability. Learners will explore case studies illustrating successful plantwide control designs, focusing on the interplay between different process units and the role of advanced control technologies. The module also discusses the importance of adaptability in control structures to accommodate process changes.

  • This module provides a systematic approach to plantwide control design, emphasizing a structured methodology for developing effective control systems. It outlines key steps in the design process, from identifying control objectives to implementing and validating control strategies. Learners will engage with example applications to solidify their understanding, exploring how systematic design can enhance process efficiency and reliability. The importance of continuous improvement and adaptation in control system design is also discussed.

  • This module introduces the Luyben design procedure, a renowned approach for developing plantwide control systems. It covers the principles and steps of the procedure, highlighting its application in various chemical processes. Learners will examine case studies demonstrating the effectiveness of the Luyben design, focusing on its ability to streamline control system development and enhance process performance. The module also discusses the advantages of using a structured design approach in complex process environments.

  • This module explores the role of equipment capacity constraints in plantwide control design. It provides insights into how capacity limitations affect control strategies and the methods for addressing these constraints. Learners will examine techniques for optimizing process operations within equipment limits, ensuring efficiency and safety. The module includes practical examples and case studies illustrating the impact of capacity constraints on control system performance and the strategies for overcoming related challenges.

  • This module presents a detailed case study of a recycle process, highlighting the challenges and solutions in plantwide control design. It covers the dynamics of recycle operations, the impact on material and energy balances, and the strategies for effective control. Learners will analyze how control systems can be tailored to manage recycle streams and enhance process stability and efficiency. The module emphasizes the importance of systematic design approaches in achieving successful control outcomes.

  • This module continues the case study on a recycle process, providing further insights into the control challenges and solutions. It explores advanced control techniques for managing complex recycle operations and the role of control systems in optimizing process performance. Learners will engage with detailed analysis and examples, understanding how to implement effective control strategies that enhance process reliability and profitability. The module underscores the importance of adaptability in control designs to accommodate process changes.

  • This module provides a comprehensive case study of a C4 isomerization process, focusing on the unique control challenges and solutions. It covers the process dynamics, the impact of isomerization on control strategies, and the methods for achieving optimal performance. Learners will explore the integration of advanced control systems to manage variations and enhance process efficiency. The module includes practical insights and examples, emphasizing the importance of tailored control solutions for complex chemical processes.

  • This module continues the C4 isomerization process case study, delving deeper into the control challenges and strategies for optimization. It discusses the role of control systems in managing process variability and achieving desired isomerization outcomes. Learners will analyze the integration of control technologies and the impact on process performance, understanding how to tailor control solutions for maximum efficiency and reliability. The module also explores the economic implications of effective control in isomerization processes.

  • This module revisits the C4 isomerization process, providing additional insights into the control strategies and optimization techniques. It covers the latest advancements in control technologies and their application in isomerization processes. Learners will examine case studies illustrating successful implementations of control systems, focusing on the benefits of enhanced process stability and efficiency. The module highlights the continuous improvement of control systems and the importance of staying updated with technological advancements.

  • This module presents a systematic economic plantwide control design procedure, focusing on maximizing profitability while ensuring process stability and safety. It outlines the steps involved in developing cost-effective control strategies, from initial design to implementation and evaluation. Learners will engage with real-world examples illustrating the economic benefits of optimized control systems. The module emphasizes the importance of balancing economic considerations with technical requirements in control system design.

  • This module provides an in-depth case study of the ethyl benzene process, highlighting the control challenges and solutions. It covers the process dynamics, the impact on control strategies, and the methods for achieving optimal process performance. Learners will explore the integration of advanced control systems to manage variations and enhance efficiency. The module includes practical insights and examples, emphasizing the importance of tailored control solutions for complex chemical processes.

  • This module revisits the C4 isomerization process, providing additional insights into the control strategies and optimization techniques. It covers the latest advancements in control technologies and their application in isomerization processes. Learners will examine case studies illustrating successful implementations of control systems, focusing on the benefits of enhanced process stability and efficiency. The module highlights the continuous improvement of control systems and the importance of staying updated with technological advancements.

  • This module contrasts conventional and top-down approaches in plantwide control design, examining their respective advantages and limitations. It discusses how these approaches influence control system development and process performance. Learners will analyze case studies demonstrating the application of both methods, understanding how to select the appropriate approach based on process requirements. The module emphasizes the importance of flexibility in control design and the benefits of integrating multiple approaches for optimal outcomes.

  • This module focuses on the plantwide control of the Cumene process, which is vital in the production of phenol and acetone. Understanding the control strategy is essential for optimizing the operation and efficiency of this chemical process. The module will cover:

    • The dynamics of the Cumene process and its key variables.
    • Control objectives and strategies employed to manage disturbances effectively.
    • Designing an effective control structure that enhances profitability.
    • Case study analysis highlighting real-world applications and challenges.

    Through this module, students and professionals will gain insights into the complexities of managing the Cumene process and develop skills in applying theoretical concepts to practical scenarios.